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Projects Hydrogel-based Phototheranostic Systems for Breast Cancer
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Hydrogel-based Phototheranostic Systems for Breast Cancer

Development of hydrogel-based phototheranostic systems with targeted photodynamic action on breast cancer.

Summary

Breast cancer is a significant health issue with high incidence worldwide. Current treatment approaches face challenges such as therapy resistance, invasiveness of biopsy, non-specific toxicity of chemotherapy, and damage to healthy tissues by radiation therapy. To overcome these challenges, the proposed project aims to develop hydrogel-based phototheranostic systems for targeted breast cancer treatment. This interdisciplinary approach combines photodynamic therapy with hydrogel drug delivery systems to provide real-time diagnosis and concurrent treatment.

The photosensitizer used is Motexafin lutetium (MLu) due to its fluorescence emission and singlet oxygen generation capabilities. Motexafin lutetium can be activated by 732 nm light, enabling deeper tissue penetration.

The project involves two stages: development and evaluation of phototheranostic systems, and characterization and in vitro evaluation of hydrogel systems. Activities include designing irradiation systems, characterizing motexafin lutetium and hydrogels, optimizing parameters, and evaluating therapeutic efficacy.

breast cancer photodynamic therapy hydrogels drug delivery motexafin lutetium singlet oxygen

Cognitive & Socio-Economic Impact

The project has generated both significant cognitive and socio-economic impact by advancing fundamental knowledge and enabling future applications in photodynamic therapy and smart biomaterials. Scientifically, it has clarified the photophysical behavior of motexafin lutetium (MLu), demonstrating a high singlet oxygen quantum yield and positioning MLu as a highly efficient photosensitizer for breast cancer phototherapy, while also establishing experimental methodologies and custom optical setups for real-time monitoring of singlet oxygen and laser-induced hydrogel photopolymerization. At the same time, the project has provided an integrated framework linking irradiation parameters, hydrogel network structure, residual photoinitiator content, and MLu release kinetics, thus defining optimal processing windows for several MLu-loaded hydrogel formulations.

Socio-economically, these results open a path toward minimally invasive, localized treatments with reduced side effects and potential cost savings for cancer care, and offer transferable know-how for other biomedical and industrial applications involving photocrosslinked hydrogels. The creation of dedicated experimental infrastructure, the training of young researchers, participation in international conferences, preparation of a scientific manuscript, and drafting of a patent application further strengthen the institution's research capacity and its potential for innovation and technology transfer.

Project Details

Contract 5TE/2025 — PN-IV-P2-2.1-TE-2023-1059
Funding MEC, ANC, UEFISCDI
Programme Research projects to stimulate young independent teams (TE)
Leader Tatiana Tozar
Contractor National Institute for Laser, Plasma and Radiation Physics (INFLPR)
Start 08.01.2025
End 31.12.2026

Expected Results

  • Characterization of MLu exposed to laser radiation, including fluorescence and singlet oxygen measurements
  • Formation of hydrogels using poly(vinyl alcohol), poly(ethylene glycol), and their combinations, through photo-polymerization
  • Evaluation of the physical and chemical properties of the hydrogels using spectroscopic techniques, microscopy, and contact angle measurements
  • Characterization of MLu hydrogel systems, including monitoring of fluorescence and singlet oxygen generation
  • Release studies of MLu from the hydrogels and evaluation of therapeutic efficacy using in vitro assays

Project Team

Contractor
National Institute for Laser, Plasma and Radiation Physics (INFLPR)
Leader Tatiana Tozar
Angela Staicu
Ionut Relu Andrei
Adriana Smarandache
Andra Dinache
Mihai Boni

Stage Reports

January 2025 – December 2025

Stage 1: Development and evaluation of phototheranostic systems.

Objectives
  1. Development and implementation of irradiation systems
  2. Evaluation of motexafin lutetium
  3. Formation of the hydrogel systems
  4. Analysis and optimization
Deliverables
  • · Design of the irradiation system for motexafin lutetium irradiation
  • · Design of the irradiation system construction for hydrogel fabrication
  • · Fluorescence data on motexafin lutetium exposed to laser radiation
  • · Singlet oxygen data on motexafin lutetium exposed to laser radiation
  • · Hydrogel-based phototheranostic systems
  • · Web page
  • · Two scientific communications – international/national conference
  • · One article in preparation
  • · Stage report
Dissemination
Articles

Article in preparation

Conferences

T. Tozar, M. Boni, S. Nistorescu, A. Staicu. “Laser-induced photo-crosslinking of hydrogel for controlled release.” E-MRS Spring Meeting 2025, Strasbourg, France 26–30 May 2025 — poster presentation.

T. Tozar, M. Boni, A. Staicu, A. Dinache. “Development and characterization of motexafin lutetium-loaded hydrogels for NIR-activated photodynamic therapy in breast cancer.” SHIFT 2025, San Cristóbal de La Laguna, Spain, 13–17 October 2025 — oral presentation.

Patents

Romanian patent application in preparation

January 2026 – December 2026

Stage 2: In-depth characterization and in vitro evaluation of phototheranostic hydrogel systems.

Objectives
  1. Characterization of phototheranostic hydrogel systems
  2. In vitro therapeutic evaluation on breast cancer cells
  3. Analysis and optimization
Deliverables
  • · Design of irradiation system for monitoring fluorescence and singlet oxygen generation
  • · Release studies of motexafin lutetium from the hydrogels
  • · Phototheranostic hydrogel systems
  • · Development of the irradiation and fluorescence monitoring system for in vitro evaluation
  • · In vitro evaluation of therapeutic efficacy of the phototheranostic hydrogel systems
  • · Two scientific communications – international/national conference
  • · Two articles in peer-reviewed journals ranked Q1
  • · Final report
  • · Project website – update

Publications

Photothermal-Responsive Polyvinyl Alcohol/Gelatin/Graphene Oxide Hydrogels Loaded with Quercetin for NIR-Triggered Controlled Drug Delivery
A. Croitoru, T. Tozar, M. Boni, A. Staicu, R. Trușcă, B. Tihăuan, A. Ficai
Gels 12(4) , 327 · 2026 doi:10.3390/gels12040327 ↗
Photopolymerization of Chlorpromazine-Loaded Gelatin Methacryloyl Hydrogels: Characterization and Antimicrobial Applications
T. Tozar, S. Nistorescu, G. Gradisteanu Pircalabioru, M. Boni, A. Staicu
Gels 10(10) , 632 · 2024 doi:10.3390/gels10100632 ↗